Optimization of Headspace-Solid Phase Microextraction (HS-SPME) technique for the analysis of volatile compounds of margarine
Küçük Resim Yok
Tarih
2019
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Springer India
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
The objective of the study was to develop optimum Headspace-Solid Phase Microextraction (HS-SPME) conditions for determining volatile compounds of margarine. the effects of fiber type, extraction temperature, extraction time on extraction rates of 2,3 butandione, dimethyl disulfide, nonanal, butanoic acid, hexanoic acid, octanoic acid, gamma-nonalactone, delta-decalactone, total area and number of volatile compounds were investigated. A response surface methodology was applied using three independent variables such as fiber type, extraction temperature and extraction time. the fiber type, extraction temperature and extraction time were arranged with Box-Behnken design. the results shows that extraction temperature and extraction time affect both total area and number of volatile compounds but fiber type effect total area of volatile compounds. the optimum HS-SPME conditions were determined as 47.54 degrees C extraction temperature and 33.63 min extraction time using DVB/CAR/PDMS fiber type.
Açıklama
Elmaci, Yesim/0000-0001-7164-838X
Anahtar Kelimeler
SPME, Optimization, Response surface methodology, Margarine, Volatile compounds
Kaynak
Journal of Food Science and Technology-Mysore
WoS Q Değeri
Q3
Scopus Q Değeri
Cilt
56
Sayı
11
