Fe3O4-SiO2-MIL-53 (Fe) nanocomposite for magnetic dispersive micro-solid phase extraction of cadmium (II) at trace levels prior to HR-CS-FAAS detection

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dc.authorscopusid7006488616
dc.authorscopusid57208524302
dc.authorscopusid58173676700
dc.authorscopusid56322932500
dc.contributor.authorSoylak, M.
dc.contributor.authorUzcan, F.
dc.contributor.authorGöktaş, O.
dc.contributor.authorGümuş, Z.P.
dc.date.accessioned2024-08-25T18:35:57Z
dc.date.available2024-08-25T18:35:57Z
dc.date.issued2023
dc.departmentEge Üniversitesien_US
dc.description.abstractA magnetic metal–organic framework Fe3O4-SiO2-MIL-53 (Fe) nanocomposite was synthesized for magnetic dispersion micro-solid phase extraction (M-d-µSPE) of cadmium in water, spice, chocolate, tea, and tobacco samples prior to the detection by flame atomic absorption spectrometry. Fe3O4-SiO2-MIL-53 (Fe) nanocomposite fabricated using the solvothermal technique was characterized using a field emission scanning electron microscope and X-ray diffraction. The extraction efficiency of the method was improved by optimizing the experimental factors. After optimization, the linearity range for Cd (II) was 4.3–500 µgL-1. The limits of detection and quantification were 1.3 and 4.3 µgL-1, respectively. The presented magnetic dispersion-micro solid phase extraction method was applied to Cd (II) analysis in food and some environmental samples. © 2023 Elsevier Ltden_US
dc.description.sponsorshipErciyes Üniversitesi: FYL-2023-12504en_US
dc.description.sponsorshipThe authors are grateful for the financial support of the Unit of the Scientific Research Projects of Erciyes University (FYL-2023-12504).en_US
dc.identifier.doi10.1016/j.foodchem.2023.136855
dc.identifier.issn0308-8146
dc.identifier.pmid37478612en_US
dc.identifier.scopus2-s2.0-85165392302en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://doi.org/10.1016/j.foodchem.2023.136855
dc.identifier.urihttps://hdl.handle.net/11454/100481
dc.identifier.volume429en_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherElsevier Ltden_US
dc.relation.ispartofFood Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz20240825_Gen_US
dc.subjectCadmiumen_US
dc.subjectFood samplesen_US
dc.subjectMetal organic frameworksen_US
dc.subjectPreconcentrationen_US
dc.subjectWater samplesen_US
dc.subjectAbsorption spectroscopyen_US
dc.subjectAtomic absorption spectrometryen_US
dc.subjectCadmium compoundsen_US
dc.subjectChemical contaminationen_US
dc.subjectDispersionsen_US
dc.subjectExtractionen_US
dc.subjectNanocompositesen_US
dc.subjectOrganometallicsen_US
dc.subjectPhase separationen_US
dc.subjectScanning electron microscopyen_US
dc.subjectSilicaen_US
dc.subjectSynthesis (chemical)en_US
dc.subjectTrace elementsen_US
dc.subject'spice'en_US
dc.subjectDispersive micro solid-phase extractionsen_US
dc.subjectFood samplesen_US
dc.subjectMagnetic metalsen_US
dc.subjectMetalorganic frameworks (MOFs)en_US
dc.subjectMicrosolidphase extractionen_US
dc.subjectPre-concentrationen_US
dc.subjectSynthesiseden_US
dc.subjectTrace levelen_US
dc.subjectWater samplesen_US
dc.subjectMagnetiteen_US
dc.subjectcadmiumen_US
dc.subjectironen_US
dc.subjectmagnetiteen_US
dc.subjectmetal organic frameworken_US
dc.subjectnanocompositeen_US
dc.subjectnanomaterialen_US
dc.subjectcadmiumen_US
dc.subjectnanocompositeen_US
dc.subjectsilicon dioxideen_US
dc.subjectArticleen_US
dc.subjectatomic absorption spectrometryen_US
dc.subjectfield emissionen_US
dc.subjectlimit of detectionen_US
dc.subjectpHen_US
dc.subjectsolid phase microextractionen_US
dc.subjectX ray diffractionen_US
dc.subjectchemistryen_US
dc.subjectmagnetismen_US
dc.subjectproceduresen_US
dc.subjectsolid phase extractionen_US
dc.subjectCadmiumen_US
dc.subjectMagnetic Phenomenaen_US
dc.subjectNanocompositesen_US
dc.subjectSilicon Dioxideen_US
dc.subjectSolid Phase Extractionen_US
dc.titleFe3O4-SiO2-MIL-53 (Fe) nanocomposite for magnetic dispersive micro-solid phase extraction of cadmium (II) at trace levels prior to HR-CS-FAAS detectionen_US
dc.typeArticleen_US

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