The Synthesis of fatty acid esters of some nitrobenzyl alcohols and investigation of their physical properties
Küçük Resim Yok
Tarih
1997
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Ege Üniversitesi
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
IV ÖZET BAZI NÎTROBENZÎL ALKOLLERİN BAZI YAĞ ASİDİ ESTERLERİNİN SENTEZİ VE FİZİKSEL ÖZELLİKLERİNİN İNCELENMESİ Nesibe TEZCAN Yüksek Lisans Tezi, Kimya Anabilim Dalı Tez Yöneticisi : Prof.Dr. Hüseyin AVCIBAŞI 1997, 50 sayfa Bu çalışmada, (m- ve p-) nitrobenzil alkollerin yağ asidi (palmitik asit ve stearik asit) esterleri ile m-nitrobenzoik asit esterleri elde edildi, jo -Nitrobenzil alkol, benzil klorürün nitrolama reaksiyonu, w -nitrobenzil alkol ise benzaldehit'in nitrolanması sonrası NaBIL* ile indirgenmesiyle elde edildi. Elde edilen ürünlerin sallandırılma işlemlerinden sonra yapılan spektroskopik yöntemlerle (İR, UV, !H-NMR ve 13C-NMR) belirlendi
ABSRTACT THE SYNTHESIS OF FATTY ACID ESTERS OF SOME NITROBENZYL ALCOHOLS AND INVESTIGATION OF THEIR PHYSICAL PROPERTIES TEZCAN, Nesibe MSc. in Chemistry SupervisorrProf.Dr.Hüseyin AVCIBAŞI 1997, 50 pages In this study, fatty acid (palmitic acid and stearic acid) and m-nitrobenzoic acid esters of (m- and p-) nitrobenzyl alcohols were synthesized. p-Nitrobenzyl alcohol was synthesized by nitration of benzyl chloride and w -nitrobenzyl alcohol was synthesized by nitration of benzaldehyde, followed by reduction with NaBK*. All products were purified by crystallisation and characterised using ^-NMR, 13C-NMR, IR and UV spectroscopy.
ABSRTACT THE SYNTHESIS OF FATTY ACID ESTERS OF SOME NITROBENZYL ALCOHOLS AND INVESTIGATION OF THEIR PHYSICAL PROPERTIES TEZCAN, Nesibe MSc. in Chemistry SupervisorrProf.Dr.Hüseyin AVCIBAŞI 1997, 50 pages In this study, fatty acid (palmitic acid and stearic acid) and m-nitrobenzoic acid esters of (m- and p-) nitrobenzyl alcohols were synthesized. p-Nitrobenzyl alcohol was synthesized by nitration of benzyl chloride and w -nitrobenzyl alcohol was synthesized by nitration of benzaldehyde, followed by reduction with NaBK*. All products were purified by crystallisation and characterised using ^-NMR, 13C-NMR, IR and UV spectroscopy.
Açıklama
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Anahtar Kelimeler
Kimya, Chemistry, Esterler, Esters, Nitrobenzil alkoller, Nitrobenzyl alcohols, Yağ asitleri, Fatty acids
