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Öğe Demineralization of cheese whey by sequential nanofiltration (NF) and electrodialysis (ED) processes(Amirkabir University of Technology - Membrane Processes Research Laboratory, 2019) Kaya, N.; Altiok, E.; Gökkaya, D.S.; Kabay, N.; Ötleş, S.In this study, demineralization of cheese whey by sequential nanofiltration (NF) and electrodialysis (ED) methods was investigated. For the NF step, two NF membranes labeled as NF-270 and NF-90 were tested. Approximately 90% of protein and lactose rejections were obtained with partial demineralization during NF step. For full demineralization of the NF permeate, NF followed by ED process. Two different ED systems (Tokuyama TS-1-10 with Neosepta membranes and Mega EDZ-10x4-0.8 with Ralex membranes) were used. The rejections of Na+, K+, Ca2+, and Mg2+ ions from the NF permeate with Ralex membranes were calculated as 82.5%, 99.3%, 87.9%, and 92.9%, while the corresponding values were 80.2%, 99.0%, 95.6%, and 100% by Neosepta membranes, respectively. © 2019 MPRL. All rights reserved.Öğe Effect of Diatomite Weight Fraction on Morphology, Thermal and Physical Properties of Diatomite Filled High Density Polyethylene Composites(Polish Acad Sciences Inst Physics, 2018) Sever, K.; Atagur, M.; Altay, L.; Seki, Y.; Uysalman, T.; Sen, I.; Kaya, N.; Guven, A.; Sarikanat, M.High density polyethylene (HDPE) has been used extensively in many sectors of the industry. The main reason for the frequent use of HDPE is its low cost, easy processing, and high performance. These sectors include household and garden products, packaging etc. In order to reduce the production cost of plastic products and to improve plastic's moldability and stability, one or more minerals are usually filled into the thermoplastics. The minerals commonly used as fillers in plastic molding compounds include calcium carbonate, talc, silica, wollastonite, clay, mica, glass beads, and alumina trihydrate. In this paper, diatomite (DA) filled HDPE composites were prepared with gelimat mixer and hot press molding technique. Thermal properties of the composites were studied by thermogravimetric analysis and dynamic mechanical analysis. The mechanical properties of the composites were determined by using universal testing machine. Morphology of the composites was investigated by scanning electron microscopy. With the addition of DA into HDPE, significant change in tensile and flexural strengths of HDPE was not observed. The loss and storage moduli increased with increasing weight fraction of DA.Öğe Fabrication and characterization of olive pomace filled PP composites(Elsevier Sci Ltd, 2018) Kaya, N.; Atagur, M.; Akyuz, O.; Seki, Y.; Sarikanat, M.; Sutcu, M.; Seydibeyoglu, M. O.; Sever, K.The aim of this study is to investigate the filling properties of an agricultural waste, olive pomace powder (OP), for polypropylene (PP) matrix material. Different weight fractions of OP (from 10 to 40 wt %), which has a median particle size of 21.36 mu m (D50) mu m, were loaded into PP by high-speed thermo kinetic mixer. In this research, the effects of weight fraction of OP within PP on mechanical, viscoelastic, thermal, chemical, crystallographic, and morphological properties of PP composites were investigated by tensile and three point bending test, dynamic mechanic analysis, thermogravimetric analysis and differential scanning calorimetry, Fourier transform infrared analysis, X-ray diffraction analysis, and scanning electron microscopy. When 40 wt% OP filler was loaded into PP, the Young's modulus and flexural modulus of PP increased by about 62.5% and 19%, respectively. The storage modulus and thermal stability of PP were remarkably enhanced with increasing OP weight fraction. (C) 2017 Elsevier Ltd. All rights reserved.Öğe Nanoscale surface modification of UltraHigh Molecular Weight Polyethylene (UHMWPE) samples with the W plus C ion implantation(Materials Research Soc, 2007) Urkac, E. Sokullu; Oztarhan, A.; Tihminlioglu, F.; Kaya, N.; Budak, S.; Chhay, B.; Muntele, C.; Oks, E.; Nikolaev, A.; Ila, D.; Ila, D; Baglin, J; Kishimoto, N; Chu, PKIn this work, Ultra High Molecular Weight Poly Ethylene (UHMWPE) samples Were implanted by W + C ions using Metal-Vapour Vacuum Arc (MEVVA) ion implantation system with a fluence of 10(17) ion/cm(2) and extraction voltage of 30 kV. Samples were characterized with Raman Spectra, ATR-FTIR, UV-VIS-NlR Spectrum and RBS. Surface morphology of implanted and unimplanted samples were examined in nanoscale with AFM.Öğe Polymeric thermal analysis of C+H and C+H+Ar ion implanted UHMWPE samples(Elsevier Science Bv, 2007) Kaya, N.; Oztarhan, Ahmet M.; Urkac, E. S.; Ila, D.; Budak, S.; Oks, E.; Nikolaev, A.; Ezdesir, A.; Tihminlioglu, F.; Tek, Z.; Cetiner, S.; Muntele, C.Chemical surface characterization of C + H hybrid ion implanted UHMWPE samples were carried out using DSC (differential scanning calorimeter) and TGA (thermal gravimetric analysis) techniques. Samples were implanted with a fluence of 10(17) ion/cm(2) and an extraction voltage of 30 kV. The study of TGA and DSC curves showed that: (1) Polymeric decomposition temperature increased, (2) T-m, Delta C-p and Delta H-m values changed while Delta C-p and Delta H-m increased. T-g value could not be measured, because of some experimental limitations. However, the increase in Delta H-m values showed that T-g values increased, (3) the branch density which indicated the increase in number of cross-link (M-c) decreased in ion implanted samples and (4) increase in Delta H-m values indicated increase in crystallinity of implanted surface of UHMWPE samples. Published by Elsevier B.V.Öğe Structural and Thermal Characterization of Ti plus O Ion Implanted UltraHigh Molecular Weight Polyethylene (UHMWPE)(Amer Inst Physics, 2009) Oztarhan, A.; Urkac, E. Sokullu; Tihminlioglu, F.; Kaya, N.; Ila, D.; Budak, S.; Chhay, B.; Muntele, C.; Oks, E.; Nikolaev, A.; McDaniel, FD; Doyle, BLIn this work, Metal-Gas Hybrid Ion Implantation technique was used as a tool for the surface modification of Ultra High Molecular Weight Polyethylene (UHMWPE). Samples were Ti + O ion implanted by using Metal-Vapour Vacuum Arc (MEVVA) ion implanter to a fluence of 5x10(16) ion/cm(2) for each species and extraction voltage of 30 kV. Untreated and surface treated samples were investigated by Rutherford Back Scattering (RBS) Spectrometry, Attenuated Total Reflectance - Fourier Transform Infrared (ATR-FTIR) Spectroscopy, Thermo Gravimetric Analysis (TGA) and Differential Scanning Calorimetry (DSC). Results indicate that Ti + O ion implantation can be applied on UHMWPE surfaces successfully. ATR-FTIR spectra indicate that the C-H concentration on the surface decreased after Ti + O implantation. Thermal characterization with TGA and DSC shows that polymeric decomposition temperature is shifted after ion implantation.Öğe Thermal characterization of Ag and Ag plus N ion implanted ultra-high molecular weight polyethylene (UHMWPE)(Elsevier Science Bv, 2007) Urkac, E. Sokullu; Oztarhan, A.; Tihminlioglu, F.; Kaya, N.; Ila, D.; Muntele, C.; Budak, S.; Oks, E.; Nikolaev, A.; Ezdesir, A.; Tek, Z.Most of total hip joints are composed of ultra-high molecular weight polyethylene (UHMWPE). However, as ultra-high molecular weight polyethylene is too stable in a body, wear debris may accumulate and cause biological response such as bone absorption and loosening of prosthesis. In this study, ultra-high molecular weight polyethylene samples were Ag and Ag + N hybrid ion implanted by using MEVVA ion implantation technique to improve its surface properties. Samples were implanted with a fluence of 10(17) ion/cm(2) and extraction voltage of 30 kV. Implanted and unimplanted samples were investigated by thermo-gravimetry analysis (TGA), differential scanning calorimetry (DSC), X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), optical microscopy (OM) and contact Angle measurement. Thermal characterization results showed that the ion bombardment induced an increase in the % crystallinity, onset and termination degradation temperatures of UHMWPE. (c) 2007 Elsevier B.V. All rights reserved.
