The effects of plasma immersion ion implantation and deposition (PIII&D) process voltages on the morphology, phase formation and E. coli adhesion of Ag coatings obtained on the surface of Ti6Al4V orthopedic implant material in nitrogen plasma [Plazma daldirma iyon implantasyonu ve biriktirme (PIII&D) prosesi gerilimlerinin azot plazmasinda ortopedik implant malzemesi Ti6Al4V yüzeyinde oluşturulan Ag kaplamalarinin morfolojilerine, faz oluşumlarina ve E. coli adezyonuna etkileri]
Küçük Resim Yok
Tarih
2017
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Gazi Universitesi Muhendislik-Mimarlik
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
In order to combine the antimicrobial effect of silver with mechanical and chemical properties of titanium nitrate, Ag was deposited on the surface of Ti6Al4V (orthopedic implant material) in N2 plasma by using plasma immersion ion implantation and deposition (PIII&D) method. The coatings were formed by using varied negative pulsed high voltage and magnetron sputtering voltage values of PIII&D process. Surface morphologies of coatings were determined with atomic force microscopy (AFM), while cross-section morphologies were determined with field emission scanning electron microscopy (FE-SEM). The phases and chemical compositions of coatings were investigated by using X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS), respectively. XPS depth profile analysis were done to reveal the penetration of Ag+ ions into the surface of specimen. In in vitro anti-bacterial effectiveness experiments, the adhesion of E. coli (Escherichia coli) microorganism, which were marked with 99mTc radioisotope, on surfaces of specimens was investigated. It was consequently determined that Ag was dominant in the coatings obtained by applying 8 kV negative pulsed high voltage, while Ag decreased on the surface depending on the increase in the voltage.
Açıklama
Anahtar Kelimeler
Plasma immersion ion implantation and deposition, Silver, Titanium nitride, X-ray photoelectron spectroscopy
Kaynak
Journal of the Faculty of Engineering and Architecture of Gazi University
WoS Q Değeri
Scopus Q Değeri
Q2
Cilt
32
Sayı
1
