Structural and thermal investigations on cerium oxalate and derived oxide powders for the preparation of (Th,Ce)O-2 pellets

dc.contributor.authorAltas, Y
dc.contributor.authorTel, H
dc.date.accessioned2019-10-27T18:19:18Z
dc.date.available2019-10-27T18:19:18Z
dc.date.issued2001
dc.departmentEge Üniversitesien_US
dc.description.abstractCe-2(C2O4)(3) . nH(2)O powder was prepared by adding oxalic acid to a cerium nitrate solution. Cerium oxalate was identified by chemical and thermal analysis, (DTA/TGA). Cerium oxalate powder was calcined to oxides at different temperatures and the powder properties (specific surface area, particle size distribution, mean particle size, bulk and tap densities) of these oxides were determined. X-ray diffraction (XRD) patterns of cerium dioxide powders obtained at different calcination temperatures were evaluated. The crystallite size was calculated both from XRD data using Sherrer's equation and from specific surface area data for each temperature. (Th0.95Ce0.05)O-2 powder was prepared by mixing the binary oxides. The compacted pellets were calcined in air at 1050 degreesC. The XRD patterns of these pellets were evaluated to characterise the formed solid solution. (C) 2001 Elsevier Science B.V. All rights reserved.en_US
dc.identifier.doi10.1016/S0022-3115(01)00655-9
dc.identifier.endpage320en_US
dc.identifier.issn0022-3115
dc.identifier.issn0022-3115en_US
dc.identifier.issue3en_US
dc.identifier.startpage316en_US
dc.identifier.urihttps://doi.org/10.1016/S0022-3115(01)00655-9
dc.identifier.urihttps://hdl.handle.net/11454/35640
dc.identifier.volume298en_US
dc.identifier.wosWOS:000171381600012en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.language.isoenen_US
dc.publisherElsevier Science Bven_US
dc.relation.ispartofJournal of Nuclear Materialsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.titleStructural and thermal investigations on cerium oxalate and derived oxide powders for the preparation of (Th,Ce)O-2 pelletsen_US
dc.typeArticleen_US

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