Schiff base-functionalised styrofoam resin for preconcentration of metal ions in wastewater and wastewater-irrigated vegetables samples

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dc.contributor.authorSiyal A.N.
dc.contributor.authorMemon S.Q.
dc.contributor.authorElçi A.
dc.contributor.authorAkdogan A.
dc.contributor.authorHol A.
dc.contributor.authorKartal A.A.
dc.contributor.authorElçi L.
dc.date.accessioned2019-10-26T21:27:15Z
dc.date.available2019-10-26T21:27:15Z
dc.date.issued2014
dc.departmentEge Üniversitesien_US
dc.description.abstractPolystyrene (PS) was extracted from styrofoam waste and functionalised with schiff base, N,N-bis(salicylidene)cyclohexanediamine (SCHD) through an azo spacer. The resin was characterised and used for preconcentration of Pb(II), Ni(II) and Cd(II) ions prior to their trace determinations by microsample injection system–coupled flame atomic absorption spectrometry (MIS-FAAS). The recoveries of studied metal ions were achieved ?96.0% with relative standard deviation (RSD) ?4.5 at optimum parameters: pH 8; resin amount 300 mg; flow rates 3.0 mL min-1 of sample solution; and 2.0 mL min-1 of eluent (2.0 mol L-1 HNO3). The limits of detection (LODs) and limits of quantification (LOQs) were found to be 0.32, 0.23 and 0.21 and 1.10, 0.78 and 0.69 µg L-1, respectively, with preconcentration factors (PFs) of 500, 800 and 1000, respectively. The linear ranges of the method were 1–40, 1–25 and 1–20 µg L-1 for Pb(II), Ni(II) and Cd(II) ions, respectively. The accuracy and validation of the method were evaluated by analysis of certified reference materials (CRMs). The method was successfully applied for preconcentration of studied metal ions in wastewater and wastewater-irrigated vegetable samples. © 2014, © 2014 Taylor & Francis.en_US
dc.description.sponsorshipThe authors would like to thank the Scientific and Technical Research Council of Turkey (TUBITAK) and Department of Chemistry, Pamukkale University, Turkey, for providing financial supports and laboratory space, respectively, for this study. --en_US
dc.identifier.doi10.1080/03067319.2014.974590
dc.identifier.endpage1477en_US
dc.identifier.issn0306-7319
dc.identifier.issn0306-7319en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage1463en_US
dc.identifier.urihttps://doi.org/10.1080/03067319.2014.974590
dc.identifier.urihttps://hdl.handle.net/11454/17401
dc.identifier.volume94en_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor and Francis Ltd.en_US
dc.relation.ispartofInternational Journal of Environmental Analytical Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectchelating resinen_US
dc.subjectMIS-FAASen_US
dc.subjectpreconcentrationen_US
dc.subjectsolid-phase extractionen_US
dc.subjectstyrofoam foam wasteen_US
dc.subjectvegetablesen_US
dc.subjectwastewater irrigationen_US
dc.titleSchiff base-functionalised styrofoam resin for preconcentration of metal ions in wastewater and wastewater-irrigated vegetables samplesen_US
dc.typeArticleen_US

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