Magnetite-molecularly imprinted polymer based highly sensitive chromatographic method for preconcentration and determination of pirimicarb

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dc.contributor.authorIlktac, Raif
dc.contributor.authorGumus, Zinar Pinar
dc.date.accessioned2020-12-01T11:58:36Z
dc.date.available2020-12-01T11:58:36Z
dc.date.issued2020
dc.departmentEge Üniversitesien_US
dc.description.abstractPesticides are harmful compounds even in trace levels for human health, so the importance of determination of these compounds is increasing day by day. Magnetite-molecularly imprinted polymer and high resolution liquid chromatography has been combined for the preconcentration and sensitive and selective determination of trace levels of pirimicarb. the developed method appeared to be rapid since the total procedure for detection of pirimicarb can be completed within one hour. the magnetic polymer is reusable and the same polymer can be used at least ten cycles for detection of pirimicarb. Limit of detection (LOD) of the method was found to be 1.60 mu g L-1 within the linear range of 7.5-250 mu g L-1. Proposed method has been applied to water and apple samples and quantitative recovery values were obtained. the proposed method appeared to be suitable for both preconcentration and determination of trace levels of pirimicarb by combining the selectivity of the reusable imprinted polymer with the high sensitivity of liquid chromatography-quadrupole-time-of-flight mass spectrometry. Magnetite-molecularly imprinted polymer combined with high resolution chromatography has been used for the first time for the determination of pirimicarb.en_US
dc.description.sponsorshipResearch Fund of Ege UniversityEge University [18-EGEMATAL-003]en_US
dc.description.sponsorshipThis work was supported by Research Fund of Ege University for financial support [Grant no: 18-EGEMATAL-003].en_US
dc.identifier.doi10.1080/03067319.2020.1804890
dc.identifier.issn0306-7319
dc.identifier.issn1029-0397
dc.identifier.issn0306-7319en_US
dc.identifier.issn1029-0397en_US
dc.identifier.scopus2-s2.0-85089174063en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.urihttps://doi.org/10.1080/03067319.2020.1804890
dc.identifier.urihttps://hdl.handle.net/11454/62063
dc.identifier.wosWOS:000556479400001en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofInternational Journal of Environmental Analytical Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectPirimicarben_US
dc.subjecthigh resolution chromatographyen_US
dc.subjectmolecularly imprinted polymeren_US
dc.titleMagnetite-molecularly imprinted polymer based highly sensitive chromatographic method for preconcentration and determination of pirimicarben_US
dc.typeArticleen_US

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