Vortex-assisted solid phase extraction on MIL-101(Cr) of parabens in waters and cosmetics by HPLC-DAD

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dc.authorscopusid55758251900
dc.authorscopusid56322932500
dc.authorscopusid54383365200
dc.authorscopusid6603631989
dc.authorscopusid7006488616
dc.contributor.authorYengin, Cigdem
dc.contributor.authorGumus, Zinar Pinar
dc.contributor.authorIlktac, Raif
dc.contributor.authorElci, Aydan
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2024-08-25T18:47:38Z
dc.date.available2024-08-25T18:47:38Z
dc.date.issued2023
dc.departmentEge Üniversitesien_US
dc.description.abstractIn this study, metal organic framework MIL-101 (Cr) was used as an adsorbent in the solid phase extraction of parabens before chromatographic analysis. Analytical parameters including pH, adsorption-desorption time, amount of adsorbent, elution solvents, desorption volume and salt effect were optimized. Optimum adsorbent amount and total adsorption and desorption time for determination of parabens were found to be 15 mg and only 10 min. The recovery values obtained with this method are in the range of 90.78-104.89% for water matrix and 85.19-108.35% for cosmetics. The detection limits of the HPLC method for methyl, ethyl, propyl, and butyl parabens are 0.0387, 0.0322, 0.0299, and 0.0339 ug/mL, respectively. Prior to HPLC analysis, a new, fast, inexpensive, and environmentally friendly solid phase extraction method based on vortex-assisted MIL-101 (Cr) adsorption was developed. This proposed VA-SPE-HPLC procedure was used for the extraction and determination of four different parabens from water and cosmetic samples.en_US
dc.description.sponsorshipUnit of the Scientific Research Projects of Erciyes University [FYL-2021-11170]; Ege University, Faculty of Pharmacy, Pharmaceutical Sciences Research Centre (FABAL)en_US
dc.description.sponsorshipThe authors are grateful for the financial support of the Unit of the Scientific Research Projects of Erciyes University (FYL-2021-11170). The authors also thank to ERU-TAUM for instrumental facilities. The authors also thank to Ege University Central Research Testing and Analysis Laboratory Research and Application Center (EGE-MATAL) and also Ege University, Faculty of Pharmacy, Pharmaceutical Sciences Research Centre (FABAL).en_US
dc.identifier.doi10.1007/s13738-023-02763-4
dc.identifier.issn1735-207X
dc.identifier.issn1735-2428
dc.identifier.scopus2-s2.0-85147944807en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.urihttps://doi.org/10.1007/s13738-023-02763-4
dc.identifier.urihttps://hdl.handle.net/11454/101991
dc.identifier.wosWOS:000930069800001en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of the Iranian Chemical Societyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz20240825_Gen_US
dc.subjectMetal organic frameworksen_US
dc.subjectParabensen_US
dc.subjectChromatographyen_US
dc.subjectWateren_US
dc.subjectCosmeticsen_US
dc.subjectPersonal-Care Productsen_US
dc.subjectLiquid-Chromatographyen_US
dc.subjectGas-Chromatographyen_US
dc.subjectPreservativesen_US
dc.subjectMicroextractionen_US
dc.subjectPreconcentrationen_US
dc.subjectAdsorbenten_US
dc.subjectSamplesen_US
dc.subjectNanoparticlesen_US
dc.subjectSorbenten_US
dc.titleVortex-assisted solid phase extraction on MIL-101(Cr) of parabens in waters and cosmetics by HPLC-DADen_US
dc.typeArticleen_US

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