Simple Magnetic Polymeric Ionic Liquid Nanocomposite Coated Hollow Fiber Membrane for the Determination of Lead (II) and Copper (II) in Water and Fruit Juice with Microinjection Sampling-Flame Atomic Absorption Spectrometry (MIS-FAAS)

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dc.authoridSalamat, Qamar/0009-0008-9455-7200
dc.authoridELCI, SUKRU GOKHAN/0000-0002-6833-6083
dc.contributor.authorSalamat, Qamar
dc.contributor.authorElci, Aydan
dc.contributor.authorElci, Sukru Gokhan
dc.date.accessioned2024-08-31T07:49:22Z
dc.date.available2024-08-31T07:49:22Z
dc.date.issued2024
dc.departmentEge Üniversitesien_US
dc.description.abstractA novel and effective adsorbent based on magnetic polymeric ionic liquid nanocomposite-coated hollow fiber membrane (MPILNC-HFM) was developed and applied for magnetic solid phase extraction of Pb (II) and Cu (II) from environmental water and fruit juice samples with microinjection sampling-flame atomic absorption spectrometry (MIS-FAAS). During extraction process, the adsorbent coated on the surface of the hollow fiber can be removed from the solution using tweezers without using a magnet. Additionally, the need to use a centrifuge during adsorption and desorption steps is also eliminated, thereby increasing the speed, simplicity, and efficiency of the extraction process. The nanocomposite characterized through Fourier-transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy-dispersive x-ray (EDX) analyses to ensure its applicability. The experimental parameters were optimized by applying one-variable-at the-time (OVAT) approach. Under optimal conditions, limits of detection were achieved 16.5 mu g L-1 for Pb (II) and 20.4 mu g L-1 for Cu (II), respectively, with relative standard deviations up to 7.9% and relative recoveries in the range of 91.8%-02.2%.en_US
dc.description.sponsorshipAdvanced Technology Application and Research Centeren_US
dc.description.sponsorshipThe authors would like to thank Turkey Scholarship program for the provided fellowship. The authors would like to thank Pamukkale University Science Faculty Department of Chemistry for allowing access to use their available instrumentation. The authors would like to thank Advanced Technology Application and Research Center (ILTAM) for SEM analysis and the interpretation of the results.en_US
dc.identifier.doi10.1080/00032719.2024.2312407
dc.identifier.issn0003-2719
dc.identifier.issn1532-236X
dc.identifier.scopus2-s2.0-85185139072en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.urihttps://doi.org/10.1080/00032719.2024.2312407
dc.identifier.urihttps://hdl.handle.net/11454/104822
dc.identifier.wosWOS:001160289500001en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor & Francis Incen_US
dc.relation.ispartofAnalytical Lettersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz20240831_Uen_US
dc.subjectHeavy Metalsen_US
dc.subjectHollow Fiber Membraneen_US
dc.subjectMagnetic Polymeric Ionic Liquiden_US
dc.subjectMagnetic Solid Phase Extraction (Mspe)en_US
dc.subjectMicroinjection Sampling Injection-Flame Atomic Absorption Spectrometry (Mis-Faas)en_US
dc.titleSimple Magnetic Polymeric Ionic Liquid Nanocomposite Coated Hollow Fiber Membrane for the Determination of Lead (II) and Copper (II) in Water and Fruit Juice with Microinjection Sampling-Flame Atomic Absorption Spectrometry (MIS-FAAS)en_US
dc.typeArticleen_US

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