Isolation and identification of esterbenzofurans from seeds of Sytrax officinalis
Küçük Resim Yok
Tarih
2002
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Ege Üniversitesi
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
Bu çalışmada Styrax Officinalis tohum yağının içerdiği esterbenzofuran bileşiklerinin izole edilmesi ve yapılarının aydınlatılması çalışılmıştır. 5-[3-(benzoyloxy)propyl]-7-methoxy-2(3',4'methylene dioxy phenyl )benzofuran (I); 5-[3-(2-methylbutanoyloxy)propyl]-7-methoxy-2(3,4'- dimethoxyphenyl) benzofuran (ÜT);5- [3 -(2-methylbutanoyioxy)propyl] - 7-methoxy-2(3 ',4' - methylenedioxyphenyl)benzofuran (IV); 5-[3-(acetoxy)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (V), 5-[3-(hyroxyl)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (VI), bileşiklerinin yapılan İD- 2D- NMR (!H, 13C, HMBC, HMQC, COSY, NOESY), HRMS, FABMS, IR ve UV spektroskopik yöntemleri kullanılarak aydınlatılmışta.Anahtar Sözcükler; Styrax; Styrax Officinalis; Esterbenzofuran; Egonol
In this thesis, isolation and structural identefication of esterbenzofuran from seeds of Styrax Officinalis has been studied. Isolated compounds were identified by İD- 2D-NMR ('H, 13C, HMBC, HMQC, COSY, NOESY), HRMS, FABMS, IR and UV spectroscopic methods ; 5-[3-(benzoyloxy)propyl]-7-methoxy-2(3',4'methylene dioxy phenyl )benzofuran (I)5-[3-(2-methylbutanoyloxy)propyl]-7-methoxy-2(3,4'- dimethoxyphenyl) benzofuran (III), 5-[3-(2-methylbutanoyloxy)propyl]-7-methoxy-2(3',4'- methylenedioxyphenyl)benzofuran (IV), 5-[3-(acetoxy)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (V), 5-[3-(hyroxyl)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (VI) Key words; Styrax; Styrax Officinalis; Esterbenzofuran; Egonol
In this thesis, isolation and structural identefication of esterbenzofuran from seeds of Styrax Officinalis has been studied. Isolated compounds were identified by İD- 2D-NMR ('H, 13C, HMBC, HMQC, COSY, NOESY), HRMS, FABMS, IR and UV spectroscopic methods ; 5-[3-(benzoyloxy)propyl]-7-methoxy-2(3',4'methylene dioxy phenyl )benzofuran (I)5-[3-(2-methylbutanoyloxy)propyl]-7-methoxy-2(3,4'- dimethoxyphenyl) benzofuran (III), 5-[3-(2-methylbutanoyloxy)propyl]-7-methoxy-2(3',4'- methylenedioxyphenyl)benzofuran (IV), 5-[3-(acetoxy)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (V), 5-[3-(hyroxyl)propyl)-7-methoxy-2-(3',4'-methylene dioxyphenyl)benzofuran (VI) Key words; Styrax; Styrax Officinalis; Esterbenzofuran; Egonol
Açıklama
Anahtar Kelimeler
Kimya, Chemistry, Egonol, Egonol, Esterbenzofuran, Esterbenzofurans, Sytrax officinalis, Sytrax officinalis, Tohum yağları, Seed oils